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1 article(s) from Mischnick, Petra

Cyanoethylation of the glucans dextran and pullulan: Substitution pattern and formation of nanostructures and entrapment of magnetic nanoparticles

Kathrin Fiege,
Heinrich Lünsdorf,
Sevil Atarijabarzadeh and
Petra Mischnick

Beilstein J. Org. Chem. 2012, 8, 551–566, doi:10.3762/bjoc.8.63

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Graphical Abstract

Figure 1: Polysaccharide structures of pullulan and dextran cyanoethylation with acrylonitrile and NaOH as ca...

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Figure 2: ATR–IR spectra of (a) dextran, 6 kDa, and cyanoethyldextrans (b–d) CED-1–3.

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Figure 3: ATR–IR spectra of (a) pullulan, 100 kDa, and cyanoethylpullulans (b–d) CEP-1–3.

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Figure 4: ¹H NMR spectra (300 MHz) of (a) CED-2 (DS_NMR(1) = 1.81) in D₂O; (b) dextran, native in D₂O; (c) CED...

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Figure 5: ¹H NMR spectra (400 MHz) of (a) CEP-2 (DS_NMR(3) = 1.31) in D₂O; (b) pullulan, native in D₂O; (c) CE...

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Figure 6: Gas chromatogram of hydrolyzed and trimethylsilylated cyanoethylglucans; (a) CED-1 (DS_GC = 0.74); (...

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Figure 7: Experimentally determined substituent distribution in the glucosyl units (glc) of cyanoethyldextran...

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Figure 8: Experimentally determined substituent distribution in the glucosyl units (glc) of cyanoethylpullula...

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Figure 9: TEM micrograph of iron oxide nanoparticles prepared from an aqueous dispersion.

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Figure 10: SEM micrographs of CEP-3 with iron oxide nanoparticles, (Table 3, entry 2).

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Figure 11: TEM micrograph of (a) uncoated iron oxide nanoparticles; (b) of CEP-3 + iron oxide nanoparticles (n...

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Figure 12: ESI Fe distribution maps of CEP-3 with iron oxide nanoparticle (Table 3, entry 1). (A) Net Fe, shown in re...

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Published 13 Apr 2012

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